Title of article
Hydroxylammonium fluorogermanates
Author/Authors
Irena Ban، نويسنده , , Matjaz Kristl، نويسنده , , Miha Drofenik، نويسنده , , Arkadij Popovi?، نويسنده ,
Issue Information
دوهفته نامه با شماره پیاپی سال 2004
Pages
5
From page
253
To page
257
Abstract
A new hydroxylammonium compound (NH3OH)2GeF6, has been synthesized by the addition of solid NH3OHF to a solution of GeO2 dissolved in 20% HF. The compound was characterized by chemical analysis and X-ray powder diffraction, the thermal decomposition was studied by thermal analysis and mass spectrometry. (NH3OH)2GeF6 crystallizes monoclinic. Two endothermic and two exothermic peaks have been observed on the DSC curve, the decomposition product at 500 °C is GeO2.
Keywords
Hydroxylammonium fluorogermanates , Mass spectroscopy , Thermal analysis , X-ray powder diffraction
Journal title
Thermochimica Acta
Serial Year
2004
Journal title
Thermochimica Acta
Record number
1196499
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