Title of article
Aqueous ammonia route to Cu1.8S with triangular and rod-like shapes
Author/Authors
Yuanfang Liu، نويسنده , , Jinbo Cao، نويسنده , , Yuanyuan Wang، نويسنده , , Jinghui Zeng، نويسنده , , Yitai Qian، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2002
Pages
4
From page
407
To page
410
Abstract
Digenite crystalline Cu1.8S was synthesized through solvothermal reaction of CuCl2·2H2O and sulfur powder at low temperature in aqueous ammonia. X-ray powder diffraction (XRD) pattern indicates Cu1.8S is cubic phase. Transmission electron microscope (TEM) shows Cu1.8S obtained at 160 °C is triangular and Cu1.8S formed at 140 °C is rod-like. X-ray photoelectron spectrum (XPS) was used to determine the composition of as prepared products. The influence of solvent and reaction temperature was investigated. Raman spectrum of Cu1.8S was recorded.
Keywords
Rod-like , Cu1.8S , Aqueous ammonia route , Triangular
Journal title
Inorganic Chemistry Communications
Serial Year
2002
Journal title
Inorganic Chemistry Communications
Record number
1315586
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