Title of article
Sonochemical synthesis of a new nano-plate lead(II) coordination polymer constructed of maleic acid
Author/Authors
Aboutorabi، نويسنده , , Leila and Morsali، نويسنده , , Ali، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2010
Pages
6
From page
2506
To page
2511
Abstract
A new nano-sized lead(II) coordination polymer of maleic acid (H2Mal), [Pb(μ7-Mal)]n (1), has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The compound 1 was structurally characterized by single-crystal X-ray diffraction. Thermal stability of nano and bulk samples of compound 1 were studied and compared with each other. After calcination of nano-sized compound 1 at 600 °C, pure phase micro-sized lead(II) oxide has been produced.
Keywords
Nano-plate , Maleic acid , Lead(II) oxide , crystal structure
Journal title
INORGANICA CHIMICA ACTA
Serial Year
2010
Journal title
INORGANICA CHIMICA ACTA
Record number
1328509
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