• Title of article

    Study of YBa2Cu3O7-x reaction kinetics by Rietveld method

  • Author/Authors

    Ferraz، Maria Cristina Comunian نويسنده , , Basso، Heitor Cury نويسنده , , Mascarenhas، Yvonne P. نويسنده ,

  • Issue Information
    روزنامه با شماره پیاپی سال 2001
  • Pages
    -24
  • From page
    25
  • To page
    0
  • Abstract
    Using a recent proposed analysis procedure for quantitative phase determination by X-ray powder diffraction, YBa2Cu3O7-x solid state formation reaction kinetics at 900 °C was studied. Although there was the presence of partial amorphous components, it was possible to determine a reaction route for the synthesis of the title compound from X-ray powder diffraction data collected at various stages of the thermal treatment and using the Rietveld method for the quantitative determination of the phase composition.
  • Keywords
    dihydrate , polymorph , Rietveld , X-ray powder diffractometry , carbamazepine
  • Journal title
    POWDER DIFFRACTION
  • Serial Year
    2001
  • Journal title
    POWDER DIFFRACTION
  • Record number

    15206