Title of article
Simple procedure for preparation of α-fluoro esters by fluorination of ester enol silyl ethers with perchloryl fluoride
Author/Authors
Fujisawa، نويسنده , , Hidehito and Takeuchi، نويسنده , , Yoshio، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2002
Pages
4
From page
173
To page
176
Abstract
Fluorination of ester enol silyl ethers in THF at room temperature using diluted perchloryl fluoride (FClO3) in the presence of ca. 0.5 M eq. of t-BuNH2 as an additive produced the corresponding α-fluoro esters in over 80% yields.
Keywords
Perchloryl fluoride , Ester enol silyl ether , ?-Fluoro ester
Journal title
Journal of Fluorine Chemistry
Serial Year
2002
Journal title
Journal of Fluorine Chemistry
Record number
1603654
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