Title of article
A reduction–boronation route to nanocrystalline titanium diboride
Author/Authors
Chen، نويسنده , , Luyang and Gu، نويسنده , , Yunle and Shi، نويسنده , , Liang and Yang، نويسنده , , Zeheng and Ma، نويسنده , , Jianhua and Qian، نويسنده , , Yitai، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2004
Pages
3
From page
231
To page
233
Abstract
Nanocrystalline titanium diboride (TiB2) has been prepared through a reduction–boronation route by using Ti powders and BBr3 as titanium and boron sources, and metallic sodium as reductant at 400 °C. X-ray powder diffraction (XRD) pattern can be indexed as hexagonal TiB2 with the lattice constants of a=3.028 and c=3.223 Å. Transmission electron microscopy images show particle morphology with average size of 15 nm. Selected area electron diffraction patterns confirm the preparation of the hexagonal TiB2.
Keywords
C. X-ray diffraction , C. Transmission electron microscopy , B. Chemical synthesis , A. Titanium diboride
Journal title
Solid State Communications
Serial Year
2004
Journal title
Solid State Communications
Record number
1762970
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