Title of article
A high-order and broadband CRAMPS experiment using z-rotational decoupling
Author/Authors
J.T and Hohwy، نويسنده , , M. and Bower، نويسنده , , P.V. and Jakobsen، نويسنده , , H.J and Nielsen، نويسنده , , N.C.، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 1997
Pages
7
From page
297
To page
303
Abstract
A novel solid-state NMR method for the combined rotation and multiple-pulse spectroscopy (CRAMPS) of homonuclear dipolar-coupled nuclei is introduced. Using a magic-sandwich sequence z-rotational decoupling, high-order truncation of the dipolar interaction is combined with improved performance under resonance offsets and spinning speeds higher than those typically used in conventional CRAMPS. The method is described using average Hamiltonian theory to third order and demonstrated experimentally by 1H CRAMPS of rigid organic solids.
Journal title
Chemical Physics Letters
Serial Year
1997
Journal title
Chemical Physics Letters
Record number
1781470
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