Title of article
Polyol mediated synthesis of nanocrystalline M3SbS3 (M=Ag, Cu)
Author/Authors
Chen، نويسنده , , Yin-di and Shen، نويسنده , , Guozhen and Tang، نويسنده , , Kaibin and Jiang، نويسنده , , Xuan and Huang، نويسنده , , Liying and Jin، نويسنده , , Yin and Qian، نويسنده , , Yitai، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2003
Pages
5
From page
509
To page
513
Abstract
A simple and convenient polyol-mediated route has been developed to produce nanocrystalline Ag3SbS3 and Cu3SbS3 from AgNO3 and Cu(NO3)2 and SbCl3 with thiourea at 197 °C. The products were characterized by X-ray powder diffraction, X-ray photoelectron spectroscopy, and transmission electron microscopy. Analysis shows that glycol agitated state and injection rate have a great effect on the purity of the final products.
Keywords
Nanostructures , chemical synthesis , Electron microscopy
Journal title
Materials Research Bulletin
Serial Year
2003
Journal title
Materials Research Bulletin
Record number
2096173
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