Title of article
Ultrasound promoted the synthesis of N-propargylic β-enaminones
Author/Authors
Martins، نويسنده , , Marcos A.P. and Rossatto، نويسنده , , Marcelo and Prola، نويسنده , , Liziê D.T. and Pizzuti، نويسنده , , Lucas and Moreira، نويسنده , , Dayse N. and Campos، نويسنده , , Patrick T. and Frizzo، نويسنده , , Clarissa P. and Zanatta، نويسنده , , Nilo and Bonacorso، نويسنده , , Helio G.، نويسنده ,
Issue Information
فصلنامه با شماره پیاپی سال 2012
Pages
5
From page
227
To page
231
Abstract
The synthesis of 14 novel N-propargylic β-enaminones from the reaction of β-alkoxy vinyltrihalomethyl[carboxyethyl] ketones [R3C(O)CHC(R1)OMe, where R3 = CF3, CCl3, CO2Et and R1 = Me, Et, Pr, Bu, i-Pent, CH2CH2CO2Me] with propargyl amines [R2NHCH2CCH, where R2 = Pr, PhCH2] is reported. Yields, solvents and reaction times needed for reaction completion, by microwave irradiation (MW), conventional thermal heating (TH) and under ultrasound irradiation (US) are compared. The best results were obtained under US irradiation in good to excellent yields (70–93%).
Keywords
enones , Enaminones , Propargyl amines , N-Propargylic ?-enaminones
Journal title
Ultrasonics Sonochemistry
Serial Year
2012
Journal title
Ultrasonics Sonochemistry
Record number
2190088
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