• Title of article

    Microwave Synthesis of Fe2O3 Nanoparticles and Its Catalyst Investigation in One-pot Synthesis of Naphthoxazinone Derivatives

  • Author/Authors

    Hashemzehi-Goonaki، A. نويسنده Department of Chemistry, Zahedan Branch, Islamic Azad University, P.O. Box 98135-978, Zahedan, Iran , , Saffari Chaleshtori، J. نويسنده 2Cellular and Molecular Research Center, School of Medicine, Shahrekord University of Medical Sciences, Shahrekord, Islamic Republic of Iran ,

  • Issue Information
    فصلنامه با شماره پیاپی 0 سال 2015
  • Pages
    9
  • From page
    385
  • To page
    393
  • Abstract
    در اين مقاله نانوساختارهاي Fe2O3با روش ساده شيميايي ستز شد. نانوذرات سنتز شده توسط پراش اشعه X ، ميكروسكوپ الكتروني روبشي، اسپكتروسكوپي مادون قرمز ومغناطيس سنج ارتعاشي نمونهبررسي شد.آناليز مغناطيس سنج ارتعاشيرفتار فرومغناطيسي نانوساختار سنتز شده را تاييد كرد. نانوساختار سنتز شده به عنوان كاتاليست اسيدي براي سنتز ستز تك مرحله اي مشتقات نفتوكسازينوناستفاده شد.
  • Abstract
    In this work firstly Fe2O3 nanoparticles were synthesized via a simple chemical method. Properties of the product were examined by X-ray diffraction pattern (XRD), Scanning electron microscope (SEM) and Fourier transform infrared (FT-IR) spectroscopy. Vibrating sample magnetometer (VSM) shows nanoparticles exhibit ferromagnetic behavior. To continue some of the 2-naphthol condensed 1,3-oxazinone derivatives employing one-pot condensation reaction in the presence of Fe2O3 nanoparticles as an acid catalyst were described. The present methodology offers several advantages, viz. high yields, clean reaction, short reaction times, recyclability of the catalyst and simple workup procedure.
  • Journal title
    Journal of NanoStructures
  • Serial Year
    2015
  • Journal title
    Journal of NanoStructures
  • Record number

    2395829

    • Link To Document
    https://search.isc.ac/dl/search/defaultta.aspx?DTC=10&DC=2395829