Title of article
A Tandem Scalable Microwave-Assisted Williamson Alkyl Aryl Ether Synthesis under Mild Conditions Document Type: Research Paper Authors
Author/Authors
Javaherian, Mohammad Department of Chemistry - Faculty of Sciences - Shahid Chamran University of Ahvaz , Kazemi, Foad Department of Chemistry - University for Advanced Studies in Basic Sciences , Zanjan , Ayati, Ebrahim Department of Chemistry - University for Advanced Studies in Basic Sciences , Zanjan , Davarpanah, Jamal Department of Chemistry - University for Advanced Studies in Basic Sciences , Zanjan , Ramdar, Mousa Department of Chemistry - University for Advanced Studies in Basic Sciences , Zanjan
Pages
13
From page
73
To page
85
Abstract
An efficient tandem synthesis of alkyl aryl ethers, including valuable building blocks of dialdehyde and dinitro groups under microwave irradiation and solvent free conditions on potassium carbonate as a mild solid base has been developed. A series of alkyl aryl ethers were obtained from alcohols in excellent yields by following the Williamson ether synthesis protocol under practical mild conditions. Scale up ability of this practical procedure is shown by the preparation of some of the valuable dialdehydes up to 50 mmole from alcohols. The method is simple, rapid, straight-forward and holds potential for further application in organic synthesis and industrial requirements.
Keywords
Tandem , scalable , Williamson ether synthesis , Alkyl tosylate , Microwave irradiation , Bis-2-nitrophenoxy akyl ether , Bis-2-formylphenoxy , alkyl ether
Journal title
Organic Chemistry Research
Serial Year
2017
Record number
2509201
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