• Title of article

    Directed Syntheses of New Quaternary Niobium Oxysulfides: Crystal Structures and Properties of K4Nb2S10O and Rb4Nb2S10O Compared to K4Nb2S11

  • Author/Authors

    Bensch، Wolfgang نويسنده , , Krause، Oliver نويسنده , , Dürichen، Peter نويسنده , , Nather، Christian نويسنده ,

  • Issue Information
    روزنامه با شماره پیاپی سال 1999
  • Pages
    -1294
  • From page
    1295
  • To page
    0
  • Abstract
    The new compounds K4Nb2S10O and Rb4Nb2S10O have been synthesized by the reaction of potassium or rubidium alkaline polychalcogenides with NbO2, Nb2O5, or mixtures of Nb and NbO. Their structures consist of discrete [Nb2Q11]4- anions (Q = O, S) built up of two face-sharing pentagonal bipyramids, which are connected via the alkali metal cations.
  • Keywords
    Structure elucidation , Oxysulfides , Niobium chalcogenides , Solid-state chemistry , Reactive flux syntheses
  • Journal title
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
  • Serial Year
    1999
  • Journal title
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
  • Record number

    83646