Title of article
Use of a recycle-type SEC method as a powerful tool for purification of thiosialoside derivatives Original Research Article
Author/Authors
Junichi Sakamoto، نويسنده , , Chiharu Takita، نويسنده , , Tetsuo Koyama، نويسنده , , Ken Hatano، نويسنده , , Daiyo Terunuma، نويسنده , , Koji Matsuoka، نويسنده ,
Issue Information
دوهفته نامه با شماره پیاپی سال 2008
Pages
5
From page
2735
To page
2739
Abstract
An efficient separation between fully acetylated thiosialoside methyl esters and fully acetylated Neu5Ac2en methyl esters was accomplished by means of a size-exclusion chromatography (SEC) method. Purity determinations and structural elucidation of the isolated compounds were performed by a combination of elemental analyses and spectroscopic analyses, including IR, 1H, and 13C NMR, and mass spectroscopic analyses.
Keywords
Thioglycosides , Sialic acid , Sialooligosaccharides , SEC purification , Glycals
Journal title
Carbohydrate Research
Serial Year
2008
Journal title
Carbohydrate Research
Record number
965611
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