Title of article
Addition of glycerol for improved methylation linkage analysis of polysaccharides
Author/Authors
John S. Kim، نويسنده , , Bradley L. Reuhs، نويسنده , , Francis Michon، نويسنده , , Raymond E. Kaiser، نويسنده , , Rasappa G. Arumugham، نويسنده ,
Issue Information
دوهفته نامه با شماره پیاپی سال 2006
Pages
4
From page
1061
To page
1064
Abstract
A presolubilization procedure with the use of glycerol is shown to be applicable for the structural analysis of polysaccharides. Neutral, acidic, high-molecular-weight and low-molecular-weight polysaccharides were solubilized in glycerol prior to methylation and subsequent linkage analysis by GC–MS. All four types of polysaccharides showed significant increases in derivatization following presolubilization as measured by recovery of partially methylated alditol acetates.
Keywords
Gas chromatography , methylation , PMAA , Linkage analysis , Polysaccharide
Journal title
Carbohydrate Research
Serial Year
2006
Journal title
Carbohydrate Research
Record number
965731
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