• Title of article

    Chelating Retardation Effect in Nickel Assisted Phosphination: Syntheses of Atropisomeric P,N Ligands

  • Author/Authors

    Fuk Yee Kwong، نويسنده , , Albert S.C. Chan، نويسنده , , Kin Shing Chan، نويسنده ,

  • Issue Information
    هفته نامه با شماره پیاپی سال 2000
  • Pages
    7
  • From page
    8893
  • To page
    8899
  • Abstract
    Ni(PPh3)2Cl2 was found to be an effective reagent in nickel assisted phosphination of biaryl O,N triflates with chlorodiphenylphosphine to yield atropisomeric P,N ligands. The chelating effect of the substrates in the reaction played an important role. Only the monodentate PPh3 rather than bidentate dppe (1,2-bis(diphenylphosphino)ethane) nickel complex was found to be an effective reagent.
  • Keywords
    N–C axial chirality , atropisomer , acyclic imide , Steric effect , twist
  • Journal title
    Tetrahedron
  • Serial Year
    2000
  • Journal title
    Tetrahedron
  • Record number

    1081405