Title of article :
Synthesis and structural analysis of new macrocycles exhibiting 3,9-dimethyl-3,9-diaryl-2,4,8,10-tetraoxaspiro[5.5]undecane units
Author/Authors :
Mirela Balog، نويسنده , , Ion Grosu، نويسنده , , Gérard Plé، نويسنده , , Yvan Ramondenc، نويسنده , , Loïc Toupet، نويسنده , , Eric Condamine، نويسنده , , Catherine Lange، نويسنده , , Corinne Loutelier-Bourhis، نويسنده , , Valérie Peulon-Agasse، نويسنده , , Elena Bogdan، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2004
Abstract :
The template synthesis of a new series of macrocycles (from monomers to tetramers) with 2,4.8,10-tetraoxaspiro[5.5]undecane units is reported. The structural analysis of the compounds is carried out using the data of high field NMR investigations, mass spectrometry studies (FAB, MALDI and ESI-MS) and the solid state X-ray diffractometry molecular structures for three compounds.
Keywords :
Ditopic ligand , Macrocycle , 3-Dioxane , X-ray diffractomatry , ESI-MS , spiro-1
Journal title :
Tetrahedron
Journal title :
Tetrahedron