Title of article
Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state
Author/Authors
Christine B. Baltus، نويسنده , , Neil J. Press، نويسنده , , Milan D. Antonijevic، نويسنده , , Graham J. Tizzard، نويسنده , , Simon J. Coles، نويسنده , , John Spencer، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2012
Pages
6
From page
9272
To page
9277
Abstract
A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki–Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4′-methylbiphenyl-4-yl)acetamide with Z′=6 and hydrogen-bonding networks of the type N–H…O in the unit cell.
Keywords
Biphenylamides , hydrogen bonds , Z? , cross coupling , X-ray crystallography , Microwaves
Journal title
Tetrahedron
Serial Year
2012
Journal title
Tetrahedron
Record number
1105106
Link To Document