Spatially resolved in situ strain measurements from an interior twinned grain in bulk polycrystalline AZ31 alloy Original Research Article

In this paper, we report for the first time, to our knowledge, spatially resolved measurements of strain gradients across a grain containing twins, located in the bulk of a polycrystalline Mg AZ31 sample. We also report orientation mapping on three parallel sections from the bulk of the sample. We use for such purpose the technique of differential-aperture X-ray microscopy (DAXM) based on synchrotron X-rays. The DAXM technique allows us to map crystallographic strains with sub-micron-sized spatial resolution. The results of this experiment confirm indirect evidence from previous experiments having less spatial resolution that important stress gradients exist in the vicinity of twin boundaries. Such a result is relevant to understanding twin growth and de-twinning, since both mechanisms are affected by stress-driven twin dislocations at the interface.