Dry sliding wear in case-hardened niobium microalloyed steels

Low-carbon steel samples containing a small addition of niobium singly or in combination with nitrogen have been carburized in a natural Titas gas atmosphere at 950 °C and 15 psi gas pressure for different time periods. At the end of the predetermined time period, the specimens were pre-cooled to 860 °C in the furnace and quenched in 10% brine. One set of the quenched specimens was tempered at a low temperature of 160 °C and the other set was sub-zero treated at −195 °C in liquid nitrogen, followed by tempering at the same tempering temperature. Surface hardness was measured by Rockwell hardness testing machine and optical microscopy was performed on etched samples. Using a pin-on-disc type apparatus, wear test was carried out under dry sliding condition to assess the beneficial effect of niobium and niobium with nitrogen on the wear properties of the carburized and hardened low-carbon steels in relation to the resulted surface hardness and microstructures. It has been found that niobium with or without nitrogen improves the wear resistance under both the heat treatment conditions. Niobium with nitrogen is more effective than niobium in improving the wear resistance. Whatever was the heat treatment condition, the wear rate of the specimens increases for all the steels as the carburizing time increases. It has also been found that samples with sub-zero treatment always have higher wear resistance than that of samples without sub-zero treatment. Niobium singly or in combination with nitrogen has been found as a modifier of the wear mechanism.