Title of article :
Enhanced accuracy in a silicon-nitride-membrane-based microcalorimeter with variation of lateral layout
Author/Authors :
Ki Sung Suh، نويسنده , , Jae Wook Kim، نويسنده , , Hyung Joon Kim، نويسنده , , Yun Daniel Park، نويسنده , , Kee Hoon Kim، نويسنده ,
Issue Information :
دوهفته نامه با شماره پیاپی سال 2009
Pages :
7
From page :
1
To page :
7
Abstract :
We report the effect of lateral designs and resultant parasitic thermal conductance on the absolute accuracy of microcalorimeters based on a silicon-nitride membrane. Thermal properties are quantified by the curve fitting scheme based on the thermal relaxation method with two thermal decay times. In the studies of various microcalorimeter layouts, the temperature dependence of errors in the absolute values of heat capacity was found to be approximately proportional to that of the thermal conductance between the isothermal platform and the temperature reservoir. Decreasing parasitic thermal conductance by modifying the lateral designs for the thermometer and heater allowed for absolute accuracies that were typically less than 5% in a temperature range between 20 and 300 K.
Keywords :
Heat capacity , Relaxation method , Silicone-nitride membrane , Microcalorimeter
Journal title :
Thermochimica Acta
Serial Year :
2009
Journal title :
Thermochimica Acta
Record number :
1198588
Link To Document :
بازگشت