Recession behavior of Lu2SiO5 under a high speed steam jet at high temperatures

Study of recession behavior of Lu2SiO5 bulk was performed in high speed steam jet with a velocity of ∼50 m/s temperature range between 1300 and 1500 °C for 100 h. X-ray results showed that no phase change was observed for all samples after steam exposure. Detailed scanning electron microscopy examinations showed some cracks formation was observed on the bulk surface for the samples of 1400 and 1500 °C. Also, porous structure was formed on the bulk surface for the samples of 1300 and 1400 °C. As for 1500 °C sample, the porous structure disappeared after exposure test. The high magnification images of 1300 °C sample showed the depletion of grain boundary glassy phase. However, for 1400 °C sample, boundary phase was formed again, and the grain growth can be identified for the sample of 1500 °C. The recession mechanism can be explained by a mass transfer of evaporated species from the bulk surface and the weight loss rate measured can be expressed by Arrhenius plot.