Preparation and characterization of iron/titanium-oxide composite particles Original Research Article

The iron/titanium-oxide composite particles have been prepared using “in-situ” hydrogen-thermal reduction method. The composites were characterized by X-ray diffraction, physical property measurement system and Mössbauer spectroscopy. The powder X-ray diffraction patterns reveal the presence of crystalline α-iron and titanium-oxide (FeTiO3/TiO2). The Mössbauer spectra of powders have been measured at room temperature, which indicated that the α-iron and the high-spin iron(II/III) components were observed. The complex permittivity and permeability of the composites have been measured using vector network analyzers. Reflection loss of the iron/titanium-oxide composite powders dispersing in epoxy resin has been calculated using measured values of complex permittivity and permeability in the frequency range of 2–12 GHz. The maximum reflection loss of −36 dB was observed at 5.0 GHz. This study shows the possibility to obtain the novel dielectric and magnetic based microwave absorbers.