Title of article :
Synthesis of nanocrystalline Ni2B via a solvo-thermal route
Author/Authors :
Xin Feng ، نويسنده , , Yu-Jun Bai، نويسنده , , Bo Lü، نويسنده , , Yong-Rui Zhao، نويسنده , , Jie Yang، نويسنده , , Jie-Ru Chi، نويسنده ,
Issue Information :
روزنامه با شماره پیاپی سال 2004
Abstract :
Nickel boride (Ni2B) nanocrystals were successfully synthesized via the reaction of NiCl2 and NaBH4 at 420 °C with benzene as solvent. The yield is about 60%. The crystals were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS). Highly crystallized Ni2B with an average size of 20 nm was obtained.
Keywords :
nickel boride , Solvo-thermal route , X-ray powder diffraction , Transmission electron microscopy , X-ray photoelectron spectra
Journal title :
Inorganic Chemistry Communications
Journal title :
Inorganic Chemistry Communications
