Title of article
Solid state preparation of CdO nano-particles by thermolysis of a precursor as compacted nanosheet
Author/Authors
Rashidi Ranjbar، Z. نويسنده Department of Chemistry, Shahid-Bahonar University of Kerman, Kerman, Iran. (P.O. Box 76169-133). , , Sheikhshoaie، I. نويسنده Department of Chemistry, Faculty of Sciences, Shahid Bahonar University of Kerman, 76169, Kerman, Islamic Republic of Iran , , Bagheri، Z. نويسنده Department of Chemistry, Shahid-Bahonar University of Kerman, Kerman, Iran. (P.O. Box 76169-133). ,
Issue Information
فصلنامه با شماره پیاپی 18 سال 2014
Pages
5
From page
409
To page
413
Abstract
A novel complex of cadmium (II) [CdL0.5(NO3)(H2O)](1), L= N,N-bis (O-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. Compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by IR, 1HNMR spectroscopy, X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The gray single crystal of compound 1 has been synthesized by slow evaporation and characterized by IR, 1HNMR spectroscopy. Then, Compound 1 in nano size was used as initial reagent to obtain nano-particles of cadmium (II) oxide at 673 K by direct calcination. The obtained CdO nano-particles were characterized by XRD pattern as well as SEM images.
Journal title
International Journal of Nano Dimension (IJND)
Serial Year
2014
Journal title
International Journal of Nano Dimension (IJND)
Record number
1435363
Link To Document