Author/Authors :
Rashidova، نويسنده , , S.Sh and Shakarova، نويسنده , , D.Sh and Ruzimuradov، نويسنده , , O.N and Satubaldieva، نويسنده , , D.T and Zalyalieva، نويسنده , , S.V and Shpigun، نويسنده , , O.A and Varlamov، نويسنده , , V.P and Kabulov، نويسنده , , B.D، نويسنده ,
Abstract :
Preparation of hybrid nanocompositional chitosan/silica sorbent was carried out. It was shown that formation of gel in sol–gel process of hydrolytic polycondensation of tetraethoxysilane (TEOS) with including of chitosan consists of two stages. Suppression of crystallization of chitosan in obtained two-phase system and changes in IR spectra are evidenced of interactions between molecules of chitosan and silanol groups of silica network. The resulting hybrid chitosan/silica sorbent was tested by high-performance liquid chromatography (HPLC).