Title of article
Synthesis and X-ray information of substituted gem-difluoroallenyl amines
Author/Authors
Shen، نويسنده , , Qilong and Chen، نويسنده , , Chbun-Hsing and Hammond، نويسنده , , Gerald B.، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2002
Pages
5
From page
131
To page
135
Abstract
An O to N substitution in 4,4-difluorobutadiene-2,3-ol-1 has been accomplished in very satisfactory yields, and without compromising the gem-difluoroallenyl integrity, using modified Mitsunobu conditions. Recrystallization of the resulting tosyl-substituted amines furnished the first X-ray crystallographic analysis of difluoroallenes.
Keywords
Fluoroallenes , Recrystallization , nucleophiles
Journal title
Journal of Fluorine Chemistry
Serial Year
2002
Journal title
Journal of Fluorine Chemistry
Record number
1603648
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