Author/Authors :
Giner، نويسنده , , José-Luis and Kiemle، نويسنده , , David and Zuniga، نويسنده , , Daniel J، نويسنده ,
Abstract :
A convenient procedure is presented whereby the chirality of isopentenyl alcohols labeled with deuterium in the 2-position can be determined by 1H NMR analysis of their chiral esters. The MTPA, MPA and O-acetylmandelate esters were investigated in a series of NMR solvents. The best results were obtained using the O-acetylmandelates in C6D6 with homodecoupling of the 1-position.
