• Title of article

    Amination of α,β-unsaturated (2-trimethylsilanylmethyl) carboxylic esters

  • Author/Authors

    Gasperi، نويسنده , , Tecla and Antonietta Loreto، نويسنده , , M and Tardella، نويسنده , , Paolo A and Gambacorta، نويسنده , , Augusto، نويسنده ,

  • Issue Information
    هفته نامه با شماره پیاپی سال 2002
  • Pages
    4
  • From page
    3017
  • To page
    3020
  • Abstract
    The reactions of (2-trimethylsilanylmethyl) α,β-unsaturated carboxylic ethyl esters with NsONHCO2Et and CaO produce, after treatment with AcOH, α-methylene N-(ethoxycarbonyl) β-amino carboxylic esters through ring opening and elimination of the trimethylsilyl group from the intermediate aziridine. By ozonization and subsequent reductive cleavage these products give the corresponding N-(ethoxycarbonyl) β-amino α-hydroxy esters.
  • Journal title
    Tetrahedron Letters
  • Serial Year
    2002
  • Journal title
    Tetrahedron Letters
  • Record number

    1651215