Title of article :
Comparison of two stationary phases for the separation of five selected polyphenols
Author/Authors :
A. and Rodrيguez-Bernaldo de Quirَs، نويسنده , , A. and Lage-Yusty، نويسنده , , M.A. and Lَpez-Hernلndez، نويسنده , , J.، نويسنده ,
Issue Information :
ماهنامه با شماره پیاپی سال 2008
Abstract :
In this study, a conventional TEKNOKROMA, Tr-015605 TRACER EXTRASIL ODS2 (25 cm × 0.4 cm, i.d. 5 μm) column and a new stationary phase TEKNOKROMA, Tr-010065 Mediterranea sea18 (15 cm × 0.4 cm, i.d. 3 μm) were compared for the separation of five phenolic compounds.
ivity, performance characteristics, analysis time and method validation were reported for both columns. A better sensitivity and performance were achieved with the novel chromatographic support. In addition the total analysis time was significantly reduced.
thod was applied to the determination of the selected polyphenols in commercial available white wines. LC–MS was used as a confirmatory technique.
Keywords :
Stationary phases , Performance characteristics , HPLC , Method validation , Polyphenols