Title of article
A solvent-free synthesis of (dichloroiodo)arenes from iodoarenes
Author/Authors
Zielinska، نويسنده , , Agnieszka and Skulski، نويسنده , , Lech، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2004
Pages
3
From page
1087
To page
1089
Abstract
An efficient solid-state oxidation of iodoarenes, ArI, is described using the urea–hydrogen peroxide adduct (UHP), a stable, inexpensive, and easily handled oxidant. The reactions were complete in 15 min at 85 °C. The melts thus obtained were reacted with excess hydrochloric acid to afford crude (dichloroiodo)arenes, ArICl2, in 64–98% yields.
Keywords
Iodoarenes , (Dichloroiodo)arenes , Solid-state oxidation , Urea–hydrogen peroxide adduct as oxidant
Journal title
Tetrahedron Letters
Serial Year
2004
Journal title
Tetrahedron Letters
Record number
1656892
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