Author/Authors :
Sloan، نويسنده , , Jeremy and Dunin-Borkowski، نويسنده , , Rafal E. and Hutchison، نويسنده , , John L. and Coleman، نويسنده , , Karl S. and Clifford Williams، نويسنده , , V. and Claridge، نويسنده , , John B. and York، نويسنده , , Andrew P.E. and Xu، نويسنده , , Cigang and Bailey، نويسنده , , Sam R. and Brown، نويسنده , , Gareth and Friedrichs، نويسنده , , Steffi and Green، نويسنده , , Malcolm L.H، نويسنده ,
Abstract :
The relative size distributions of molecules of C60 and higher fullerenes observed in single walled carbon nanotubes (SWNTs) produced by arc vaporization of carbon in the presence of a mixed Ni/Y catalyst are described. The experimental and calculated imaging properties of the fullerenes, which were observed in ca. 5–10% of SWNTs, are also described. The in situ e-beam irradiation in a 300 kV field emission gun transmission electron microscope causes rapid coalescence of the fullerenes within the SWNTs. The incorporated fullerenes also directly impede crystal growth in SWNTs when their cavities are filled by the liquid phase capillary method.
Keywords :
C60 , carbon , FEGTEM , Fullerenes , Nanotubes , SWNTs , TEM , crystallisation