Title of article :
One-pot synthesis of N-allylthioureas using supported reagents
Author/Authors :
Aoyama، نويسنده , , Tadashi and Murata، نويسنده , , Sumiko and Nagata، نويسنده , , Yasutaka and Takido، نويسنده , , Toshio and Kodomari، نويسنده , , Mitsuo، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2005
Abstract :
A simple and efficient method has been developed for the synthesis of N-allylthioureas from allylic bromides in one-pot by using a supported reagents system, KSCN/SiO2–RNH3OAc/Al2O3, in which allyl bromide reacts first with KSCN/SiO2 and the product, allyl isothiocyanate, reacts with RNH3OAc/Al2O3 to give the final product, N-allylthiourea, in good yield.
Keywords :
Thiourea , supported reagents , one-pot synthesis
Journal title :
Tetrahedron Letters
Journal title :
Tetrahedron Letters