Title of article
Fast preparation of dihydrocyclocitral from citronellal under solventless microwave irradiation
Author/Authors
Doan، نويسنده , , Nhuan Ngoc and Le، نويسنده , , Thach Ngoc and Hansen، نويسنده , , Poul Erik and Duus، نويسنده , , Fritz، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2005
Pages
3
From page
6749
To page
6751
Abstract
Dihydrocyclocitral, a useful reagent in organic synthesis, has been synthesized in high yield and with high stereoselectivity from citronellal under microwave irradiation in two steps, involving acetic anhydride under base catalysis, then p-toluenesulfonic acid adsorbed on silica gel under solventless conditions (80% yield, reaction time 22 min).
Keywords
Solventless synthesis , Isomeric selectivity , Dihydrocyclocitral , Citronellal , microwave irradiation , solid support
Journal title
Tetrahedron Letters
Serial Year
2005
Journal title
Tetrahedron Letters
Record number
1846758
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