Title of article
Chromatography-free product separation in the Mitsunobu reaction
Author/Authors
Proctor، نويسنده , , Anthony J. and Beautement، نويسنده , , Kevin and Clough، نويسنده , , John M. and Knight، نويسنده , , David W. and Li، نويسنده , , Yingfa Li، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2006
Pages
4
From page
5151
To page
5154
Abstract
Mitsunobu products can be isolated pure without column chromatography by first washing a solution of the crude reaction mixture in dichloromethane with 15% aqueous hydrogen peroxide followed by aqueous sodium sulfite. A final filtration through silica gel secures the pure Mitsunobu product.
Journal title
Tetrahedron Letters
Serial Year
2006
Journal title
Tetrahedron Letters
Record number
1851363
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