Title of article
Synthesis of 1,4-diazepin-5-ones under microwave irradiation and their reduction products
Author/Authors
Wlodarczyk، نويسنده , , Nicolas and Gilleron، نويسنده , , Pauline and Millet، نويسنده , , Régis and Houssin، نويسنده , , Raymond and Hénichart، نويسنده , , Jean-Pierre، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2007
Pages
4
From page
2583
To page
2586
Abstract
A new efficient access to 1,4-diazepane derivatives is described via a microwave assisted synthesis of 7-substituted-1,4-diazepin-5-ones, which proceeds rapidly in good yields. Catalytic reduction gave 1,4-diazepan-5-ones and 1,4-diazepanes whereas a ring opening was observed by hydride reduction when a phenyl group occupies the N-benzylic position.
Keywords
4-Diazepin-5-one , 1 , 1 , Ethanediamine , microwave irradiation , 4-Diazepane
Journal title
Tetrahedron Letters
Serial Year
2007
Journal title
Tetrahedron Letters
Record number
1854679
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