Title of article
Synthesis and properties of a new SASRIN resin derivative: SASRIN–2-pyridylthiocarbonate (SASRIN–TOPCAT) resin
Author/Authors
Zhao، نويسنده , , Peng and Yang، نويسنده , , Zhen-Jun and Zhang، نويسنده , , Liangren and Zhang، نويسنده , , Li-He، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2008
Pages
5
From page
2951
To page
2955
Abstract
A new SASRIN resin derivative, SASRIN–TOPCAT resin, was synthesized by the reaction of SASRIN resin with 2-thiopyridyl chloroformate. The new resin can be used for the loading of alcohols and thiols under neutral conditions, and the release of alcohol from the resin is achieved by the treatment of 1% TFA in CH2Cl2 for 15–60 min. Compared to the other reported resins, SASRIN–TOPCAT resin is more suitable for the loading of alcohols in solid-phase organic synthesis.
Keywords
SASRIN resin derivative , etherification , solid-phase organic synthesis
Journal title
Tetrahedron Letters
Serial Year
2008
Journal title
Tetrahedron Letters
Record number
1859096
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