Title of article :
2,2,3,3,11,11,12,12-Octamethyl-1,4,7,10,13-pentaoxacyclohexadecane: improved synthesis and crystal structure with NaSCN
Author/Authors :
Loustau-Chartez، نويسنده , , Fanny and Robeson، نويسنده , , Rachel M. and Custelcean، نويسنده , , Radu and Sachleben، نويسنده , , Richard A. and Bonnesen، نويسنده , , Peter V.، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2009
Abstract :
An efficient synthesis of 2,2,3,3,11,11,12,12-octamethyl-1,4,7,10,13-pentaoxacyclohexadecane (1, OM16C5) is described, which affords over an order of magnitude improvement in yield over the previously reported method. The first X-ray crystal structure of 1, as a complex with NaSCN, is also reported.
Keywords :
Crown ether , 16-Crown-5 , sodium , improved synthesis
Journal title :
Tetrahedron Letters
Journal title :
Tetrahedron Letters
