Title of article :
Efficient syntheses of 3H-azuleno[8,1-cd]pyridazines and their thermal and photochemical reactions
Author/Authors :
Wu، نويسنده , , Chi-Phi and Devulapally، نويسنده , , Rammohan and Li، نويسنده , , Tsung-Chieh and Ku، نويسنده , , Chien-Kuo and Chung، نويسنده , , Hsien-Chung، نويسنده ,
Issue Information :
هفته نامه با شماره پیاپی سال 2010
Abstract :
Azulenopyridazines 6 were efficiently synthesized from ethyl 4-hydrazinylazulene-1-carboxylate (2) by p-toluenesulfonic acid-catalyzed imine formation and intramolecular cyclization followed by dehydrogenation using KOH/MeOH in one-pot operation. Thermal and photochemical reactions of azulenopyridazines 6 afforded 1-vinylazulenes 7 in good yields.
Keywords :
Azulene , Azulenopyridazine , p-Toluenesulfonic acid , Thermal reaction , Photochemical reaction
Journal title :
Tetrahedron Letters
Journal title :
Tetrahedron Letters
