Title of article
Oxidation of disulfides with Selectfluor™: concise syntheses of thiosulfonates and sulfonyl fluorides
Author/Authors
Kirihara، نويسنده , , Masayuki and Naito، نويسنده , , Sayuri and Ishizuka، نويسنده , , Yuki and Hanai، نويسنده , , Honoka and Noguchi، نويسنده , , Takuya، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2011
Pages
4
From page
3086
To page
3089
Abstract
The reaction of aromatic or benzylic disulfides with 2.5 equiv of Selectfluor™ in acetonitrile/water (10:1) at room temperature efficiently produced the corresponding thiosulfonates. On the other hand, the reaction of disulfides with 6.5 equiv of Selectfluor™ in refluxing acetonitrile/water (10:1) provided sulfonyl fluoride in high yields.
Keywords
Selectfluor™ , disulfide , Thiosulfonate , Sulfonyl fluoride , Oxidation
Journal title
Tetrahedron Letters
Serial Year
2011
Journal title
Tetrahedron Letters
Record number
1878489
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