Title of article
Synthesis and resolution of 2-hydroxyhexahelicene
Author/Authors
Mourad and Ben Braiek، نويسنده , , Mourad and Aloui، نويسنده , , Faouzi and Ben Hassine، نويسنده , , Béchir، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2013
Pages
3
From page
424
To page
426
Abstract
2-Hydroxyhexahelicene has been prepared in good yield and purity via a three-step sequence involving palladium-catalysed Heck coupling and classical oxidative photocyclisation reactions. The two enantiomers of this hexacyclic helicenol have been separated using (S)-(−)-camphanoyl chloride as the chiral resolving agent.
Keywords
helicenes , Enantiomeric resolution , Heck coupling , Photocyclisation
Journal title
Tetrahedron Letters
Serial Year
2013
Journal title
Tetrahedron Letters
Record number
1883516
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