Title of article
Synthesis and characterization of metal-free phthalocyanine containing 16-membered N2S2-donor macrocycles linked to a 2-pyridinyl methyl moiety
Author/Authors
Kabay، نويسنده , , Nilgün and G?k، نويسنده , , Ya?ar، نويسنده ,
Issue Information
هفته نامه با شماره پیاپی سال 2013
Pages
5
From page
4086
To page
4090
Abstract
A metal-free phthalocyanine (H2Pc) containing four diazadithiamacrocycles a with 2-pyridinyl methyl groups attached was synthesized via cyclotetramerization of 4,5-bis{2-[13(2-pyridinylmethyl)-1,9-dithia-5,13-diazacyclohexadecanyl-5]ethyl} thiophthalonitrile in the presence of DBU as a strong organic base. New compounds were characterized by a combination of elemental analysis, 1H NMR, 13C NMR, IR, UV/vis, and MS spectral data.
Keywords
Metal-free phthalocyanine , Mixed donor macrocycle , Macrocyclization , Detosylation , Pendant arms
Journal title
Tetrahedron Letters
Serial Year
2013
Journal title
Tetrahedron Letters
Record number
1885078
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