Title of article :
THE CRYSTAL AND MOLECULAR STRUCTURE OF 2-HYDROXYBENZYALDEHYDE O, O (1, 4-DIOXOBUTANE-1, 4-DIYL) OXIME, C16H13N2O6
Author/Authors :
ETEMADI، B نويسنده 1Dept. of Earth Sciences, Shiraz University, Shiraz, I. R. of Iran, , , TAEB، A نويسنده Dept. of Chemical Engineering, Iran University of Science and Technology, Tehran, I. R. of Iran , , SHARGHI، H نويسنده 5Dept. of Chemistry, Shiraz University, Shiraz, I. R. of Iran , , TAJARODI، A نويسنده Dept. of Chemical Engineering, Iran University of Science and Technology, Tehran, I. R. of Iran , , HOSSEINI، M نويسنده 5Dept. of Chemistry, Shiraz University, Shiraz, I. R. of Iran ,
Issue Information :
دوفصلنامه با شماره پیاپی 0 سال 2006
Abstract :
C16H13N2O6, Mr=239.30, Monoclinic, P21/n, a=7.6088(3), b=9.0108 (4), c=11.2161(6)
??A
,
B =100.3633(4) ?? , V=759.90(6)
??A
3, Z=2, Dx=1.446g/cm3, Dm=1.450g/cm3, ? (MoK? )=0.71007
??A,
T=293K, R=0.044, Rw=0.043 for 1295 observed reflections. The crystals were prepared by slow evaporation
technique. A directed hydrogen bond is associated with the asymmetric part of the molecule between O1---H1
... N1 of 2.601
??A
. The ring system is planar and the molecules are held together by vander Waals forces.
Journal title :
Iranian Journal of Science and Technology Transaction A: Science
Journal title :
Iranian Journal of Science and Technology Transaction A: Science
