Title of article
Sonochemical syntheses and characterization of nano-structured three-dimensional lead(II) coordination polymer constructed of fumaric acid
Author/Authors
Aboutorabi، نويسنده , , Leila and Morsali، نويسنده , , Ali، نويسنده ,
Pages
5
From page
407
To page
411
Abstract
Nano-structured three-dimensional lead(II) coordination polymer, [Pb(μ6-Fum)]n (1); {Fum = Fumarate}, has been synthesized by sonochemical method and characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. Solvent effects on size and morphology of nano-structured compound 1 have been studied. Calcination of the nano-sized compound 1 at 600 °C under air atmosphere yields PbO nanoparticles. The thermal stability of compound 1 both its bulk and nano-size has been studied by thermal gravimetric (TG) and differential thermal (DTA) analyses and compared each other.
Keywords
Lead(II) oxide , Nano-particles , Fumaric acid , Coordination polymers
Journal title
Astroparticle Physics
Record number
2007005
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