Author/Authors :
Wang، نويسنده , , X.Q. and Xu، نويسنده , , D and Cheng، نويسنده , , X.F. and Lu، نويسنده , , M.K. and Yuan، نويسنده , , D.R. and Huang، نويسنده , , J and Lu، نويسنده , , G.W and Ning، نويسنده , , H.X and Duan، نويسنده , , X.L. and Wang، نويسنده , , Z.M. and Lu، نويسنده , , G.T and Li، نويسنده , , S.G. and Chen، نويسنده , , Y and Zhou، نويسنده , , Y.Q، نويسنده ,
Abstract :
The synthesis and purification of zinc mercury thiocyanate, ZnHg(SCN)4 (ZMTC), are described. The identity of the synthesized compound was characterized by elemental analysis, X-ray powder diffraction, infrared, Raman, and UV/Vis/NIR transmission spectra. The thermal stability and thermal decomposition of ZMTC crystal were investigated by means of thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) measurements. The intermediates and final products of the thermal decomposition were identified by X-ray powder diffraction (XRPD).
Keywords :
C. thermogravimetric analysis (TGA) , C. Raman spectroscopy , C. Infrared spectroscopy , C. Differential scanning calorimetry (DSC) , C. X-ray diffraction
