Title of article
Synthesis of nanocrystalline Mn3O4 at 100 °C
Author/Authors
Anilkumar، نويسنده , , M. and Ravi، نويسنده , , V.، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2005
Pages
5
From page
605
To page
609
Abstract
A simple gel to crystal conversion route has been followed for the preparation of nanocrystalline tetragonal Mn3O4 powders at 80–100 °C under refluxing conditions. Freshly prepared manganese hydroxide gel is allowed to crystallize under refluxing and stirring conditions for 4–6 h. Formation of nano crystallites of Mn3O4 is confirmed by X-ray diffraction (XRD) study. Transmission electron microscope (TEM) investigations revealed that the average particle size is 50 nm for these powders.
Keywords
A. Ceramics , A. Oxides , C. X-ray diffraction , C. Electron microscopy , B. Chemical synthesis
Journal title
Materials Research Bulletin
Serial Year
2005
Journal title
Materials Research Bulletin
Record number
2097067
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