Title of article
Controllable synthesis and characterization of cadmium molybdate octahedral nanocrystals by coprecipitation method
Author/Authors
Shahri، نويسنده , , Zahra and Sobhani، نويسنده , , Azam and Salavati-Niasari، نويسنده , , Masoud، نويسنده ,
Issue Information
روزنامه با شماره پیاپی سال 2013
Pages
9
From page
3901
To page
3909
Abstract
Cadmium molybdate (CdMoO4) nanocrystals have been successfully synthesized via coprecipitation method by using Cd(Sal)2 (Sal = salicylidene) and (NH4)6Mo7O24·4H2O as starting materials in water as solvent. Effects of temperature, reaction time, solvent, surfactant and cadmium source were investigated to reach optimum condition. It was found that particle size, morphology and phase of the final products could be greatly influenced via these parameters. The products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectra, photoluminescence (PL) spectroscopy, energy dispersive X-ray microanalysis (EDX), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).
Keywords
B. Chemical synthesis , C. X-ray diffraction , D. Optical properties , A. Nanostructures , A. Inorganic compounds
Journal title
Materials Research Bulletin
Serial Year
2013
Journal title
Materials Research Bulletin
Record number
2104176
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