Title of article :
Microwave Assisted Eco-friendly Synthesis of Chalcones using 2,4-dihydroxy Acetophenone and Aldehydes as Corrosion Inhibitors for Mild Steel in 1M HCl
Author/Authors :
Verma، Chandra Bhan نويسنده Department of Chemistry, Indian Institute of Technology, Banaras Hindu University, Varanasi 221005, India Verma, Chandra Bhan , Reddy، Mareddy Jayanth نويسنده Department of Metallurgical Engineering, Indian Institute of Technology, Banaras Hindu University, Varanasi 221005. India Reddy, Mareddy Jayanth , Quraishi، Mumtaz Ahmad نويسنده Department of Chemistry, Indian Institute of Technology, Banaras Hindu University, Varanasi 221005, India Quraishi, Mumtaz Ahmad
Issue Information :
دوماهنامه با شماره پیاپی 0 سال 2014
Pages :
20
From page :
321
To page :
340
Abstract :
In the present investigation we have synthesized four chalcones namely 3-(4- chlorophenyl)-1-(2, 4-dihydroxyphenyl) prop-2-en-1-one (CHAL-1), 1-(2, 4- dihydroxyphenyl)-3-p-tolylprop-2-en-1-one (CHAL-2) 1-(2, 4-dihydroxyphenyl)-3-(2- hydroxyphenyl) prop-2-en-1-one (CHAL-3) and 1-(2, 4-dihydroxyphenyl)-3-(4-hydroxy-3- methoxyphenyl) prop-2-en-1-one (CHAL-4) and premeditated their corrosion inhibition property on mild steel (MS) in 1M HCl using chemical and electrochemical methods. The scanning electron microscopic (SEM) study reveals the formation of protective film of chalcones on MS surface. Presence of elements on MS surface was also studied using high energy dispersive (EDX) technique. Potentiodynamic polarization study reveals that chalcones are of mixed type inhibitors. Weight –loss experiment also performed at different temperature in order to derive thermodynamic parameters and to explain mechanism of adsorption
Journal title :
Analytical and Bioanalytical Electrochemistry
Serial Year :
2014
Journal title :
Analytical and Bioanalytical Electrochemistry
Record number :
2230062
Link To Document :
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