Author/Authors :
Soltanianfard، M. J. نويسنده Department of Chemistry, Faculty of Chemical Science, Firoozabad Branch, Islamic Azad University, Firoozabad, Fars, P.O. Box 74715-117, Islamic Republic of Iran , , Firoozadeh، A. نويسنده Department of Chemistry, Faculty of Chemical Science, Firoozabad Branch, Islamic Azad University, Firoozabad, Fars, P.O. Box 74715-117, Islamic Republic of Iran ,
Abstract :
CuO nano particles were obtained by calcination of nano-sized [Cu(C4H4O4)(bipy)(H2O)2].2H2O (1) and [Cu(2‚2?-bipy)](C4H4O4)0.5(NO3)(H2O) (2) which are two Cu(II) coordination polymers. The two coordination polymers [Cu(C4H4O4)(bipy)(H2O)2].2H2O and [Cu(2‚2?-bipy)](C4H4O4)0.5(NO3)(H2O) were synthesized and characterized by Fourier transform infrared spectra (FT-IR spectroscopy), thermal gravimetric (TGA) and differential thermal analyses (DTA). CuO nano particles were characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM).The two coordination polymers obtained possessed nano sizes.
