Title of article :
Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14,16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e,-l] [1, 4] dioxacyclotridecin-15(7H)-one
Author/Authors :
بنايي عليرضا نويسنده , كريمي سهيلا نويسنده - , نورباقري نگار نويسنده Department of Chemistry, Payame Noor University, P.O. BOX 19395-4697 Tehran, Iran Nurbageri Negar
Issue Information :
فصلنامه با شماره پیاپی سال 2016
Abstract :
New 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l][1, 4] dioxacyclotridecin-15 (7H)-one(2a) was synthesized in good yield by the Petrenko-Kritchenko reaction of 2, 2ʹ-((3-hydroxypropane-1, 2-diyl) bis-(oxy)) bisbenzaldehyde(1a) with diethyl ketone in the mixture of ethanol and acetic acid as solventin the presence of ammonium acetate. The compounds were characterized by elemental analyses, IR, 1H-NMR, 13C-NMR and mass spectrometry.
Journal title :
Astroparticle Physics
