Title of article
Microwave assisted oxidation coupling of thiols to symmetrical disulfides with tripropylammonium fluorochromate (VI) (TPAFC)
Author/Authors
Hasanzadeh, Neda Faculty of Science - Islamic Azad University - Ahvaz Branch , Ghammamy, Shahriare Department of Chemistry - Faculty of Science - Imam Khomeini International University , Mohammadi, Mohammad Kazem Faculty of Science - Islamic Azad University - Ahvaz Branch
Pages
6
From page
155
To page
160
Abstract
Tripropylammonium fluorochromate(VI) (TPAFC), is an efficient and new reagent, which is
prepared easily and oxidizes thiols to the corresponding disulfides, quickly. The reactions are
performed cleanly and are controlled to stop at the disulfide stage, without over-oxidation and
side products. Coupling of thiols to their corresponding disulfides, are studied in solution at
room temperature and in solution under microwave radiation. The easy procedure, simple workup,
short reaction times, and excellent yields, are another advantages of this reagent.
Keywords
Thiol , Oxidation , Coupling , Disulfide , Tripropylammonium fluorochromate , Microwave irradiation
Journal title
Astroparticle Physics
Serial Year
2010
Record number
2437720
Link To Document